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A binary operation \\(\\sigma\\) on \\({\\mathcal P}_n\\) is a matrix connection of order \\(n\\) if it is monotone, continuous from above, and satisfies \\[ X^*(A\\,\\sigma\\,B)X\\le(X^*AX)\\,\\sigma\\,(X^*BX) \\] for all \\(A,B\\in{\\mathcal P}_n\\), \\(X\\in{\\mathcal M}_n\\). An operator connection \\(\\sigma\\) is a matrix connection of every order. Its representing function is the unique operator monotone function \\(f_\\sigma:\\mathbb{R}_+\\to\\mathbb{R}_+\\) satisfying \\[ f_\\sigma(t)I=I\\sigma(tI),\\quad t>0. \\] The dual of \\(\\sigma(\\ne 0)\\) is the operator connection \\(\\sigma^\\perp\\), defined by \\[ A\\,\\sigma^\\perp\\,B=(B^{-1}\\,\\sigma\\,A^{-1})^{-1} \\] for \\(A,B>0\\), and extended by continuity to \\(A,B\\ge 0\\). The theory of operator connections is due to \\textit{F. Kubo} and \\textit{T. Ando} [Math. Ann. 246, 205--224 (1980, Zbl 0412.47013)].  The present authors establish eigenvalue and singular value inequalities involving operator connections. Their main result (Theorem 3.1.(a)) is the following. Let \\(A,B\\in{\\mathcal P}_n\\), let \\(C\\in{\\mathcal M}_n\\) be Hermitian or symmetric, and let \\(\\sigma,\\tau,\\rho\\,(\\ne 0)\\) be operator connections. If \\(f_\\sigma^2(t)\\le f_\\tau(t)f_\\rho(t)\\), \\(t>0\\), then \\[ s_1((A\\,\\tau^\\perp\\,B)^\\frac{1}{2}\\,C^*(A\\,\\sigma\\,B)^\\sim C\\,(A\\,\\rho^\\perp\\,B)^\\frac{1}{2}) \\le\\lambda_1(AC^*B^\\sim C). \\] Here, \\(s_1\\) and \\(\\lambda_1\\) denote the largest singular value and eigenvalue, respectively, and the notation \\(X^\\sim\\) stands for \\(X\\) or \\(X^T\\).  As a consequence, the authors extend or refine results of themselves [Linear Algebra Appl. 547, 19--31 (2018; Zbl 1390.15062)], \\textit{T. Ando} [Linear Algebra Appl. 223--224, 57--64 (1995; Zbl 0829.15010)], \\textit{G. Visick} [Linear Algebra Appl. 223--224, 731--744 (1995; Zbl 0833.15019)] and \\textit{L. 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