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If \\((M,g)\\) is an \\(m\\)-dimensional Riemannian manifold such that there exists a compact set \\(K\\subset M\\) and a diffeomorphism \\(M\\setminus K\\cong(1,\\infty)\\times L\\), with  \\[ g=dr\\otimes dr+r^2g_L+0(1)\\qquad \\text{as } r\\to\\infty,\\tag{1} \\]  then we say that \\((M,g)\\) is asymptotically conical with link \\((L,g_L)\\).  If \\(k\\geq 0\\) is an integer, it is said that the expansion (1) holds in \\(C^k\\) if  \\[ \\sum_{l=0}^kr^l|\\nabla^l(g-g_C)|=0(1)\\qquad \\text{as } r\\rightarrow\\infty. \\]  Here \\(\\nabla\\) is the Levi-Civita connection of the cone \\((C,g_C)\\) where \\(C=(0,\\infty)\\times L\\) and \\(g_C=dr\\otimes dr+r^2g_L\\), and norms are computed with respect to \\(g_C\\). Similarly, given \\(\\alpha\\in (0,1)\\), it is said that the expansion (1) holds in \\(C^{k,\\alpha}\\) if the weighted \\(C^{k,\\alpha}\\) norms of \\(g-g_C\\) tends to zero as \\(r\\to\\infty\\).  In this paper the authors study the isoperimetric structure of asymptotically conical manifolds \\((M,g)\\) of dimension \\(m\\) whose link \\((L, g_L)\\) satisfies the conditions:   (2) \\(\\mathrm{Ric}_L\\geq (m-2)g_L\\);   (3) \\(\\mathrm{Area}(L,g_L)<\\omega_{m-1}\\), where \\(\\omega_{m-1}\\) is the volume of the unit sphere.  The results of this paper are the following:  Theorem 1. Let \\((M,g)\\) be an asymptotically conical manifold of dimension \\(m\\) such that the expansion (1) holds in \\(C^{2,\\alpha}\\) and with \\(\\lambda_1(-\\triangle_L)>(m-1)\\). There are \\(\\delta>0\\) and \\(V_0>0\\) such that the following hold: Let \\(V>V_0\\). Let \\(r>1\\) be such that \\(\\mathcal{L}^m_g(B_r)=V\\). There is exactly one \\(u_V\\in C^{2,\\alpha}(L)\\) with \\(-\\delta\\leq u_V\\leq\\delta\\), such that \\(\\Sigma_V=\\{(r(1+u_V(x)),x):x\\in L\\}\\) is a CMC surface that encloses volume \\(V\\). Moreover, \\(\\Sigma_V\\) is volume-preserving, the surfaces \\(\\{\\Sigma_V\\}_{V>V_0}\\) form a foliation of the complement of a compact subset of \\(M\\), and the \\(C^{2,\\alpha}\\) norms of \\(u_V\\) tend to zero as \\(V\\to \\infty\\).  Theorem 3. Let \\((M,g)\\) be an asymptotically conical manifold of dimension \\(m\\) whose link \\((L,g_L)\\) satisfies conditions (2) and (3) and such that the expansion (1) holds in \\(C^{1,\\alpha}\\). There is \\(V_0>0\\) with the following property: For every \\(V>V_0\\) there is an isoperimetric region of volume \\(V\\). Every such region \\(\\Omega_V\\) is regular and close to \\(B_r\\) where \\(r>1\\) is such that \\(\\mathcal{L}_g^m(B_r)=V\\). If the expansion (1) holds in \\(C^{2,\\alpha}\\), then \\(\\partial\\Omega_V=\\Sigma_V\\), where \\(\\Sigma_V\\) is as in Theorem 1. In particular, \\(\\Omega_V\\) is the unique isoperimetric region of volume \\(V\\).  For related papers see [\\textit{G. Huisken} and \\textit{S.-T. Yau}, Invent. Math. 124, No. 1--3, 281--311 (1996; Zbl 0858.53071); the second author et al., Invent. Math. 197, No. 3, 663--682 (2014; Zbl 1302.53037); Invent. Math. 194, No. 3, 591--630 (2013; Zbl 1297.49078); J. Differ. Geom. 94, No. 1, 159--186 (2013; Zbl 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