Anomalies in the analysis of calibrated data

DOI10.1080/00949650701756864zbMATH Open1169.62001arXivmath/0703550OpenAlexW2147839706WikidataQ57447148 ScholiaQ57447148MaRDI QIDQ3636728FDOQ3636728

Donald R. Jensen, Donald E. Ramirez

Publication date: 29 June 2009

Published in: Journal of Statistical Computation and Simulation (Search for Journal in Brave)

Abstract: This study examines effects of calibration errors on model assumptions and data--analytic tools in direct calibration assays. These effects encompass induced dependencies, inflated variances, and heteroscedasticity among the calibrated measurements, whose distributions arise as mixtures. These anomalies adversely affect conventional inferences, to include the inconsistency of sample means; the underestimation of measurement variance; and the distributions of sample means, sample variances, and Student's t as mixtures. Inferences in comparative experiments remain largely intact, although error mean squares continue to underestimate the measurement variances. These anomalies are masked in practice, as conventional diagnostics cannot discern irregularities induced through calibration. Case studies illustrate the principal issues.

Full work available at URL: https://arxiv.org/abs/math/0703550

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zbMATH Keywords

diagnosticscase studiesdirect calibrationinduced dependenciesnon-standard distributions

Mathematics Subject Classification ID

Multivariate analysis (62H99)

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Cited In (4)

• Outlier detection under star-contoured errors
• Seeking outlying subsets under star-contoured errors
• Irregularities inX(Y) fromY(X) in linear calibration
• Concentration reversals in ridge regression

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